Development and Validation of Novel Cell-free Direct Neutralization Assay for SARS-CoV-2

Publication date: Jul 25, 2024

Neutralizing antibody titer elicited through infection or vaccination is accepted as a reliable surrogate for protection from SARS-CoV-2 infection, hospitalization, and mortality. The gold standard for measuring neutralizing antibody levels relies on culturing live virus in the presence of a target cell and quantitating the level where 50% of the target cells are infected. These assays have numerous technical challenges, not the least is the requirement for a BSL-3 laboratory to perform the live virus testing. We developed the Q-NAb IgG Test for the quantitative determination of neutralizing antibodies against SARS-CoV-2 variants, traceable to WHO International Standards. The test utilizes a novel Fusion Protein that mimics the Spike receptor binding domain docked to the human ACE2 protein and effectively blocks non-neutralizing antibodies in the sample. After pre-blocking sequesters the non-neutralizing antibodies from the samples, direct binding of the residual neutralizing antibodies to variant RBDs coated in the wells of the microtiter plate is measured with a fluorescent secondary antibody. Results of the Q-NAb IgG Test agree with a live virus Microneutralization Assay for both the Ancestral strain (WA1-2020) and the Omicron BA.5 (COR-22-063113/2022) variant (Spearmans correlation, {rho} = 0.87 and 0.92, respectively). The analytical performance (LoB, LoD, LoQ, linearity, precision, and interference) of the Q-NAb IgG Test was established along with sensitivity and specificity using a panel of monoclonal neutralizing and non-neutralizing anti-SARS-CoV-2 antibodies. Clinical sensitivity and specificity using pre-pandemic, convalescent, and vaccinated serum and plasma samples is also reported. The advantages of the Q-NAb IgG Test are its strong correlation to live virus neutralization tests, traceability to WHO International Standards, convenient microtiter plate format, low sample volume requirements, and suitability for a BSL-2 laboratory.

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Concepts Keywords
Antibiotic Ace2
Donkey Ancestral
Snnldskvggnynylyrlfrksnlkpferdisteiyqagstpcngvegfncyfplqsygfqptngvgy Assay
Vaccine3 Ba
Cov
Igg
International
Kit
Medrxiv
Nab
Neutralizing
Preprint
Rbd
Sars
Titer

Semantics

Type Source Name
disease IDO cell
disease IDO assay
disease VO antibody titer
disease MESH infection
disease VO vaccination
disease MESH SARS-CoV-2 infection
pathway REACTOME SARS-CoV-2 Infection
drug DRUGBANK Gold
drug DRUGBANK Esomeprazole
disease VO Rho
disease VO vaccinated
disease VO volume
drug DRUGBANK Coenzyme M
disease VO titer
disease MESH Emergency
disease VO vaccine
disease VO time
disease VO organization
disease VO vaccine efficacy
disease VO effective
disease IDO site
drug DRUGBANK Amino acids
drug DRUGBANK Sodium Chloride
drug DRUGBANK Glycerin
drug DRUGBANK Biotin
disease VO efficiency
drug DRUGBANK Sodium lauryl sulfate
drug DRUGBANK Potassium Chloride
disease VO protocol
disease IDO blood
disease VO Comirnaty
disease VO USA
drug DRUGBANK Methylergometrine
disease VO viability
drug DRUGBANK Nitrogen
drug DRUGBANK Immune Globulin Human
disease VO manufacturer
drug DRUGBANK Amber
drug DRUGBANK Trehalose
drug DRUGBANK Mannitol
drug DRUGBANK Polysorbate 80
drug DRUGBANK Phosphate ion
disease VO dose
disease MESH uncertainty
disease IDO process
drug DRUGBANK Glutamic Acid
drug DRUGBANK Glycine
drug DRUGBANK L-Cysteine
drug DRUGBANK Serine
drug DRUGBANK L-Tyrosine
disease IDO production
disease VO population
disease VO report
disease VO manufacturing

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